An official website of the United States government.

Official websites use .gov
A .gov website belongs to an official government organization in the United States.

Secure .gov websites use HTTPS
A lock ( ) or https:// means you've safely connected to the .gov website. Share sensitive information only on official, secure websites.

Research Publications (Food Safety)

This page tracks research articles published in national and international peer-reviewed journals. Recent articles are available ahead of print and searchable by Journal, Article Title, and Category. Research publications are tracked across six categories: Bacterial Pathogens, Chemical Contaminants, Natural Toxins, Parasites, Produce Safety, and Viruses. Articles produced by USDA Grant Funding Agencies (requires login) and FDA Grant Funding Agencies (requires login) are also tracked in Scopus.

Displaying 76 - 100 of 501

  1. An Improved Stir Fabric-Phase Sorptive Extraction Combined with Ultra-High-Performance Liquid Chromatography–Tandem Mass Spectrometry Analysis for the Determination of 48 Pesticide Residues in Vegetable Samples

    • Food Analytical Methods
    • Fabric-phase sorptive extraction (FPSE) coats organic–inorganic hybrid sorbent materials onto flexible and hydrophilic fabrics through sol–gel sorbent-coating technology. Herein, we explored four different coating chemistries, including those of nonpolar sol–gel poly(dimethylsiloxane), medium polar sol–gel poly(tetrahydrofuran), and polar sol–gel poly(ethylene glycol) (PEG)–block-poly(propylene glycol)–PEG, and sol–gel PEG.

      • Chemical contaminants
      • Pesticide residues
      • Produce Safety
      • Ethylene Sensitive
  2. A Natural Deep Eutectic Solvent–based Ultrasound-Vortex-assisted Dispersive Liquid–Liquid Microextraction Method for Ligand-less Pre-concentration and Determination of Traces of Cadmium Ions in Water and Some Food Samples

    • Food Analytical Methods
    • A very explicate and ligand-less ultrasound-vortex-assisted dispersive liquid–liquid microextraction (US-VA-DLLME) technique has been designed for the pre-concentration and extraction of ultra-trace amounts of cadmium ions, before its determination by graphite furnace atomic absorption spectrophotometry.

      • Chemical contaminants
      • Heavy Metals
  3. A Natural Deep Eutectic Solvent–based Ultrasound-Vortex-assisted Dispersive Liquid–Liquid Microextraction Method for Ligand-less Pre-concentration and Determination of Traces of Cadmium Ions in Water and Some Food Samples

    • Food Analytical Methods
    • Abstract  

      • Heavy Metals
      • Chemical contaminants
  4. Utilization of Spectrochemical Analysis and Diffuse Optical Techniques to Reveal Adulteration of Alike Fish Species and Their Microbial Contamination

    • Food Analytical Methods
    • Abstract

  5. Screening Method for the Detection of Other Allergenic Nuts in Cashew Nuts Using Chemometrics and a Portable Near-Infrared Spectrophotometer

    • Food Analytical Methods
    • Nuts and peanuts are foods that are rich in minerals, vitamins, fibre and healthy fats in addition to antioxidant compounds. However, these food products can be subject to adulterations and fraud mainly due to their cost or contamination as a result of improper handling. Different types and degrees of damage can be caused to consumers due to food fraud, highlighting the serious consequences that can occur when the adulterant is toxic or allergenic.

  6. Polycyclic Aromatic Hydrocarbons (PAHs) Sample Preparation and Analysis in Beverages: A Review

    • Food Analytical Methods
    • The monitoring of food contaminants is of interests to both food regulatory bodies and the consumers. This literature review covers polycyclic aromatic hydrocarbons (PAHs) with regard to their background, sources of exposures, and occurrence in food and environment as well as health hazards. Furthermore, analytical methods focusing on the analysis of PAHs in tea, coffee, milk, and alcoholic samples for the last 16 years are presented.

      • Chemical contaminants
  7. Colorimetric Detection of Benzoyl Peroxide in the Flour Samples Based on the Morphological Transition of Silver Nanoprisms

    • Food Analytical Methods
    • In this paper, a simple and effective strategy was designed for colorimetric sensing of benzoyl peroxide (BPO) based on the morphological transition of silver nanoprisms (AgNPRs). The decomposition of O–O bond of BPO generated strong oxidant benzoyl oxide free radical, which could be first oxidized the silver atoms at the corner areas and the {110} facet of AgNPRs.

  8. An Improved Stir Fabric-Phase Sorptive Extraction Combined with Ultra-High-Performance Liquid Chromatography–Tandem Mass Spectrometry Analysis for the Determination of 48 Pesticide Residues in Vegetable Samples

    • Food Analytical Methods
    • Fabric-phase sorptive extraction (FPSE) coats organic–inorganic hybrid sorbent materials onto flexible and hydrophilic fabrics through sol–gel sorbent-coating technology. Herein, we explored four different coating chemistries, including those of nonpolar sol–gel poly(dimethylsiloxane), medium polar sol–gel poly(tetrahydrofuran), and polar sol–gel poly(ethylene glycol) (PEG)–block-poly(propylene glycol)–PEG, and sol–gel PEG.

      • Pesticide residues
      • Chemical contaminants
      • Produce Safety
      • Ethylene Sensitive
  9. Ringer Tablet-Based Micelle-Mediated Extraction-Solvent Back Extraction Coupled with High-Performance Liquid Chromatography for Preconcentration and Determination of Neonicotinoid Pesticides

    • Food Analytical Methods
    • Ringer tablet-based micelle-mediated extraction-solvent back extraction method coupled to HPLC has been investigated for the determination of neonicotinoid pesticides in honey, cucumber, and orange samples. The method employs the entrapment of the analytes in the micelles of non-ionic surfactant (Triton X-114). By ultrasonication, the ringer tablet is dissolved, and the extractant is released into the aqueous phase as very tiny droplets to provide a cloudy solution.

      • Pesticide residues
      • Chemical contaminants
  10. Rapid Detection of Escherichia coli O157:H7 by Loop-Mediated Isothermal Amplification Coupled with a Lateral Flow Assay Targeting the z3276 Genetic Marker

    • Food Analytical Methods
    • The most commonly reported serotype of Shiga toxin-producing Escherichia coli (STEC) is O157:H7. This pathogen presents a threat to public health and is a cause of foodborne illness worldwide. The efficient and sensitive detection of E. coli O157:H7 remains a challenge for food safety. In this report, we developed a sensitive and specific loop-mediated isothermal amplification (LAMP) reaction coupled with a lateral flow (LF) assay to rapidly detect E. coli O157:H7.

      • Escherichia coli O157:H7
      • Bacterial pathogens
  11. Discovery of Natural Veterinary Herbal Medicine Products in Commercial Cow Milk by Using Nontargeted Profiling on LC–ESI–TOF Platform

    • Food Analytical Methods
    • For centuries, herbal medicines have been used to treat humans and animals. Veterinary medicines are well-regulated; inspectors monitor milk and associated dairy products to screen for unacceptable contaminants. However, few scholars have discussed how the by-products of veterinary herbal medicine can be found in food products.

  12. Sensing Platform Based on Carbon Paste Electrode Modified with Bismuth Oxide Nanoparticles and SWCNT for Submicromolar Quantification of Honokiol

    • Food Analytical Methods
    • Honokiol is neolignan present in the magnolia bark. It displays versatile pharmacological properties—neuroprotective and anxiolytic effect, anti-cancer activity and antimicrobial effect being the most important. This paper aims to develop a voltammetric non-enzymatic biosensor for honokiol detection, quantification and monitoring in drugs and cosmetic products. The materials used in this study were synthesized and characterized by HR-XRPD, SEM, ATR-FTIR and electrochemical methods.

  13. A Programmed, Autonomous, and Self-powered DNA Motor for One-Step Amplification Detection of Ochratoxin A

    • Food Analytical Methods
    • A programmed, autonomous, and self-powered DNA motor was developed for one-step amplification detection of ochratoxin A (OTA). The OTA can bind with the aptamer of hairpin and induce the opening of hairpin. Then, the Mg2+-specific DNAzyme can circularly cleave the fluorophore-labeled DNA on the gold nanoparticles (AuNPs), causing autonomous and processive movement of DNA motor.

      • Mycotoxins
      • Natural toxins
  14. Correction to: Dilution of QuEChERS Extracts Without Cleanup Improves Results in the UHPLC-MS/MS Multiresidue Analysis of Pesticides in Tomato

    • Food Analytical Methods
      • Pesticide residues
      • Chemical contaminants
  15. Advances in Analysis of Contaminants in Foodstuffs on the Basis of Orbitrap Mass Spectrometry: a Review

    • Food Analytical Methods
    • Abstract

      • Antibiotic residues
      • Pesticide residues
      • Chemical contaminants
  16. Saltatory Rolling Circle Amplification-Based Ratiometric Electrochemical Biosensor for Rapid Detection of Salmonella enterica serovar Typhimurium in Food

    • Food Analytical Methods
    • Salmonella enterica serovar Typhimurium (S. enterica ser. Typhimurium) is one of the main causes of human bacterial gastroenteritis. Therefore, there is an urgent need to develop a highly specific and accurate method for S. enterica ser. Typhimurium detection in food. In the study, we constructed a ratiometric electrochemical biosensor based on saltatory rolling circle amplification (SRCA) and dual-signal electrochemical readout.

      • Salmonella
      • Bacterial pathogens
  17. Application of Ambient Ionization Mass Spectrometry to Detect the Mycotoxin Roquefortine C in Blue Cheese

    • Food Analytical Methods
    • Harmful secondary metabolites produced by fungi, mycotoxins, are found worldwide in a multitude of products. Roquefortine C (ROQ-C) is a mycotoxin produced by Penicillium roqueforti, the major fungus used to ripen blue-veined cheeses. To facilitate the screening of cheeses for ROQ-C, a method based upon the ambient ionization technique of direct analysis in real time-mass spectrometry (DART-MS) was developed.

  18. Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES): a Powerful Analytical Technique for Elemental Analysis

    • Food Analytical Methods
    • Abstract

  19. Hyperbranched Gold Plasmonic Blackbodies Enhanced Immunochromatographic Test Strip for the Sensitive Detection of Aflatoxin B1 in Maize Sample

    • Food Analytical Methods
    • In this work, we synthesized a novel hyperbranched Au plasmonic blackbody (AuPB) and applied it as a signal amplification label in immunochromatographic test strip (ICTS) sensor for the sensitive detection of aflatoxin B1 (AFB1) in maize.

      • Aflatoxins
      • Natural toxins
  20. Novel Single Primer Isothermal Amplification Method for the Visual Detection of Vibrio parahaemolyticus

    • Food Analytical Methods
    • As a typical halophilic bacterium, Vibrio parahaemolyticus (V. parahaemolyticus) is regarded as one of the marine seafood-borne pathogens causing severe illnesses in humans and aquatic animals. Herein, a novel single primer isothermal amplification (SPIA) technique which was modified with SYBR Green II was successfully developed for the visual detection of V. parahaemolyticus.

      • Vibrio
      • Bacterial pathogens
  21. Recent Progresses on Biosensors for Escherichia coli Detection

    • Food Analytical Methods
    • Foodborne illnesses caused by Escherichia coli (E. coli) are causing worldwide morbidity and mortality, threating human health. One way to limit and eliminate E. coli infections is developing fast and sensitive methods for detection. Biosensors have emerged to complement traditional strategies for E. coli detection. This review aims at providing an updated summary of developed biosensors for specific detection of E. coli in the last 5 years.

      • Bacterial pathogens
  22. Comparison of ISO 6579–1, VIDAS Easy SLM, and SureFast® Salmonella ONE Real-time PCR, for Salmonella Detection in Different Groups of Foodstuffs

    • Food Analytical Methods
    • In the European Union (EU), Salmonella was the causative agent responsible for almost one in three (30.7%) of all foodborne outbreaks reported by member states during 2018, causing 11,581 cases of illness, which represented an increase of 20.6% compared to 2017.

      • Salmonella
      • Bacterial pathogens
  23. Development of a Sandwich Enzyme-linked Immunosorbent Assay (ELISA) for the Detection of Egg Residues in Processed Food Products

    • Food Analytical Methods
    • Food allergy has become an important food safety concern affecting people’s health and quality of life. As one of the most common allergic foods, egg poses a safety hazard to susceptible individuals. Therefore, it is crucial to develop rapid and sensitive detection methods for allergen monitoring. Sandwich ELISA detection method was developed based on two polyclonal antibodies for the detection of egg white allergens in this study.

  24. Determination of 72 Chemical Pesticides and Estimation of Measurement of Uncertainty in Rice Using LC-MS/MS and GC-MS/MS

    • Food Analytical Methods
    • A multi-residue method was developed and validated for the simultaneous determination of 39 and 33 chemical pesticides in rice using LC-MS/MS and GC-MS/MS, respectively. The coefficient of determination was 0.994 to 0.999 over the linear concentration range of 0.01 to 0.1 μg mL-1. The LOD and LOQ were in the range of 0.31 to 3.35 and 1.04 to 10.06 μgkg-1, repsectively.

      • Pesticide residues
      • Chemical contaminants
  25. Antibiotic-Based Magnetic Nanoprobes Combined with mPCR for Simultaneous Detection of Staphylococcus aureus and Bacillus cereus

    • Food Analytical Methods
    • Sensitive, simple, and rapid pathogen separation and detection methods are essential for the early diagnosis and immediate medical treatment of bacterial infections. In this study, a novel strategy based on vancomycin (Van)-modified ovalbumin (OVA) mediated magnetic nanoprobes (MBs-OVA-Van) combined with multiplex polymerase chain reaction (mPCR) was developed for efficient isolation and detection of Staphylococcus aureus (S. aureus) and Bacillus cereus (B.

      • Staphylococcus aureus
      • Bacterial pathogens
      • Bacillus cereus